Information card for entry 7201548

Structure parameters

• Formula: C24 H14 O14 Pb4
• Calculated formula: C24 H12 O14 Pb4
• Title of publication: An eight-connected 3D lead(ii) metal‒organic framework with octanuclear lead(ii) as a secondary building unit: synthesis, characterization and luminescent property
• Authors of publication: Yang, En-Cui; Li, Jian; Ding, Bin; Liang, Qing-Qing; Wang, Xiu-Guang; Zhao, Xiao-Jun
• Journal of publication: CrystEngComm
• Year of publication: 2008
• Journal volume: 10
• Journal issue: 2
• Pages of publication: 158
• a: 15.282 ± 0.002 Å
• b: 13.589 ± 0.001 Å
• c: 14.027 ± 0.001 Å
• α: 90°
• β: 112.611 ± 0.001°
• γ: 90°
• Cell volume: 2689 ± 0.4 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0507
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.1296
• Weighted residual factors for all reflections included in the refinement: 0.1321
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No