Information card for entry 7201912

Structure parameters

• Formula: C65 H94 Cl4 N4 O29.25 Pd2 Zn4
• Calculated formula: C65 H86 Cl4 N4 O29.25 Pd2 Zn4
• Title of publication: Complexes as metalloligands in network formation: synthesis and characterisation of a mixed-metal coordination network containing palladium and zinc
• Authors of publication: Burrows, Andrew D.; Mahon, Mary F.; Wong, Claudia T. F.
• Journal of publication: CrystEngComm
• Year of publication: 2008
• Journal volume: 10
• Journal issue: 5
• Pages of publication: 487
• a: 13.51 ± 0.0001 Å
• b: 27.37 ± 0.0002 Å
• c: 27.991 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10350.2 ± 0.15 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0769
• Residual factor for significantly intense reflections: 0.0627
• Weighted residual factors for significantly intense reflections: 0.1716
• Weighted residual factors for all reflections included in the refinement: 0.1847
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No