Crystallography Open Database

Information card for entry 7202100

7202099 << 7202100 >> 7202101

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Coordinates	7202100.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H50 N21 Ni2 O9 P2
Calculated formula	C32 H51 N21 Ni2 O9 P2
Title of publication	Hydrogen-bonded assembly of [Ni(Im)6]2+ ion and phosphorus anions: Different sandwiched-type/tessellate-type supramolecular architectures and 1D water chains
Authors of publication	Chen, Shuo-ping; Li, Ming; Xiao, Yong; Yuan, Yi-xuan; Pan, Ling-ling; Yuan, Liang-jie
Journal of publication	CrystEngComm
Year of publication	2008
Journal volume	10
Journal issue	9
Pages of publication	1227
a	9.9153 ± 0.001 Å
b	12.8275 ± 0.0013 Å
c	20.407 ± 0.002 Å
α	76.501 ± 0.002°
β	88.539 ± 0.001°
γ	68.8 ± 0.002°
Cell volume	2348.1 ± 0.4 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	273 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0505
Residual factor for significantly intense reflections	0.0376
Weighted residual factors for significantly intense reflections	0.1166
Weighted residual factors for all reflections included in the refinement	0.1234
Goodness-of-fit parameter for all reflections included in the refinement	1.093
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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