Information card for entry 7204415

Structure parameters

• Formula: C17 H24 O6
• Calculated formula: C17 H24 O6
• Title of publication: Synthetic studies on CP-225,917 and CP-263,114: concise synthesis of the bicyclic core using an intramolecular Mukaiyama aldol reactionElectronic supplementary information (ESI) available: crystal data for 13a. See http://www.rsc.org/suppdata/p1/b2/b202752f/
• Authors of publication: Armstrong, Alan; Critchley, Trevor J.; Gourdel-Martin, Marie-Edith; Kelsey, Richard D.; Mortlock, Andrew A.
• Journal of publication: Journal of the Chemical Society, Perkin Transactions 1
• Year of publication: 2002
• Journal issue: 11
• Pages of publication: 1344
• a: 13.582 ± 0.007 Å
• b: 11.418 ± 0.006 Å
• c: 11.111 ± 0.007 Å
• α: 90°
• β: 105.71 ± 0.06°
• γ: 90°
• Cell volume: 1658.7 ± 1.7 ų
• Cell temperature: 220 ± 2 K
• Ambient diffraction temperature: 220 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.11
• Residual factor for significantly intense reflections: 0.0638
• Weighted residual factors for significantly intense reflections: 0.11
• Weighted residual factors for all reflections included in the refinement: 0.139
• Goodness-of-fit parameter for all reflections included in the refinement: 1.18
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No