Information card for entry 7207998

Structure parameters

• Formula: C18 H48 Cu9 I14 N6 O9 Tb
• Calculated formula: C18 H48 Cu9 I14 N6 O9 Tb
• Title of publication: Solid-state structural transformations in metal organic-inorganic hybrids constructed from terbium(iii) complexes and iodocuprate clusters
• Authors of publication: Mishra, Shashank; Jeanneau, Erwann; Ledoux, Gilles; Daniele, Stéphane
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 11
• Pages of publication: 3894
• a: 13.83 ± 0.02 Å
• b: 13.83 ± 0.02 Å
• c: 61.5 ± 0.4 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 10187 ± 7 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 167
• Hermann-Mauguin space group symbol: R -3 c :H
• Hall space group symbol: -R 3 2"c
• Residual factor for all reflections: 0.1156
• Residual factor for significantly intense reflections: 0.0632
• Weighted residual factors for all reflections: 0.1363
• Weighted residual factors for significantly intense reflections: 0.0709
• Weighted residual factors for all reflections included in the refinement: 0.0671
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No