Information card for entry 7208687

Structure parameters

• Common name: (Ni(Ni(5,5'dmbpy)(H2O))8(W(CN)8)6)*8H2O
• Chemical name: {Ni[Ni(5,5'dmbpy)(H2O)]8[W(CN)8]6}*8H2O
• Formula: C148 H89 N65 Ni9 O12 W6
• Calculated formula: C148 H89 N65 Ni9 O12 W6
• Title of publication: Geometrical isomerism in pentadecanuclear high-spin Ni9W6 clusters with symmetrical bidentate ligands detected
• Authors of publication: Nowicka, Beata; Stadnicka, Katarzyna; Nitek, Wojciech; Rams, Michał; Sieklucka, Barbara
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 20
• Pages of publication: 6559
• a: 19.899 ± 0.005 Å
• b: 20.113 ± 0.005 Å
• c: 31.475 ± 0.005 Å
• α: 89.305 ± 0.005°
• β: 90.024 ± 0.005°
• γ: 73.132 ± 0.005°
• Cell volume: 12054 ± 5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1964
• Residual factor for significantly intense reflections: 0.0955
• Weighted residual factors for significantly intense reflections: 0.2047
• Weighted residual factors for all reflections included in the refinement: 0.2551
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No