Information card for entry 7211228

Structure parameters

• Formula: C14 H14 Cl N5 O3 Pb
• Calculated formula: C14 H14 Cl N5 O3 Pb
• Title of publication: Solid state structural transformation of 1D to intermediate 2D and then to 3D porous coordination polymer by anion replacement; new precursors for preparation of PbCl2, Pb3O2Cl2 and PbO nanoparticles
• Authors of publication: Hashemi, Lida; Morsali, Ali
• Journal of publication: CrystEngComm
• Year of publication: 2013
• Journal volume: 15
• Journal issue: 44
• Pages of publication: 8894
• a: 14.0972 ± 0.0011 Å
• b: 8.2977 ± 0.0008 Å
• c: 15.9525 ± 0.0014 Å
• α: 90°
• β: 104.203 ± 0.007°
• γ: 90°
• Cell volume: 1809 ± 0.3 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.107
• Residual factor for significantly intense reflections: 0.0777
• Weighted residual factors for significantly intense reflections: 0.1703
• Weighted residual factors for all reflections included in the refinement: 0.1821
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No