Information card for entry 7211826

Structure parameters

• Formula: C28 H32 Cl2 N4 O85 Pr4 W12
• Calculated formula: C28 H32 Cl2 N4 O85 Pr4 W12
• Title of publication: High-dimensional frameworks dependent on coordination mode of ligand controlled by acidity of reaction solution. Syntheses, structures, magnetic and fluorescence properties of eight new compounds
• Authors of publication: Hu, Mi-Xia; Chen, Ya-Guang; Zhang, Chun-Jing; Kong, Qing-Jiao
• Journal of publication: CrystEngComm
• Year of publication: 2010
• Journal volume: 12
• Journal issue: 5
• Pages of publication: 1454
• a: 11.615 ± 0.005 Å
• b: 14.312 ± 0.005 Å
• c: 16.048 ± 0.005 Å
• α: 69.908 ± 0.005°
• β: 72.805 ± 0.005°
• γ: 86.786 ± 0.005°
• Cell volume: 2390.3 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1203
• Residual factor for significantly intense reflections: 0.0813
• Weighted residual factors for significantly intense reflections: 0.1538
• Weighted residual factors for all reflections included in the refinement: 0.1717
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No