Crystallography Open Database

Information card for entry 7213021

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Coordinates	7213021.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H42 Mn N3 O2
Calculated formula	C38 H42 Mn N3 O2
Title of publication	Enantioselective α-amination of ketones mediated by chiral nitridomanganese(V) complexes using ammonia as the terminal nitrogen source
Authors of publication	Svenstrup, Niels; Bøgevig, Anders; Hazell, Rita G.; Jørgensen, Karl Anker
Journal of publication	Journal of the Chemical Society, Perkin Transactions 1
Year of publication	1999
Journal issue	11
Pages of publication	1559
a	10.2919 ± 0.0008 Å
b	12.0062 ± 0.0009 Å
c	14.139 ± 0.001 Å
α	88.543 ± 0.001°
β	76.608 ± 0.001°
γ	77.637 ± 0.001°
Cell volume	1659.7 ± 0.2 Å³
Cell temperature	120 K
Ambient diffraction temperature	120 K
Number of distinct elements	5
Space group number	1
Hermann-Mauguin space group symbol	P 1
Hall space group symbol	P 1
Residual factor for significantly intense reflections	0.052
Weighted residual factors for significantly intense reflections	0.057
Goodness-of-fit parameter for significantly intense reflections	2.79
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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