Information card for entry 7213593

Structure parameters

• Formula: C12 H87 Fe6 Ge3 K N12 O107 W24
• Calculated formula: C2 H10 Fe6 Ge3 K N2 O104 W24
• Title of publication: Syntheses, structures and properties of two multi-iron‒samarium/multi-iron substituted germanotungstates
• Authors of publication: Wang, Jun; Zhao, Jun-Wei; Zhao, Hai-Yan; Yang, Bai-Feng; He, Huan; Yang, Guo-Yu
• Journal of publication: CrystEngComm
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 2
• Pages of publication: 252
• a: 20.7644 ± 0.0004 Å
• b: 25.0049 ± 0.0006 Å
• c: 22.6513 ± 0.0005 Å
• α: 90°
• β: 100.729 ± 0.002°
• γ: 90°
• Cell volume: 11555.2 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1123
• Residual factor for significantly intense reflections: 0.0667
• Weighted residual factors for significantly intense reflections: 0.166
• Weighted residual factors for all reflections included in the refinement: 0.1867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No