Information card for entry 7213776

Structure parameters

• Formula: C68 H48 Cu4 Ge Mo12 N12 O42 V2
• Calculated formula: C68 H48 Cu4 Ge Mo12 N12 O42 V2
• Title of publication: The design, syntheses and characterization of a series of hybrids based on polyoxometalates and metal complexes
• Authors of publication: Wang, La-Mei; Wang, Yan; Fan, Yong; Xiao, Li-Na; Hu, Yang-Yang; Gao, Zhong-Min; Zheng, Da-Fang; Cui, Xiao-Bing; Xu, Ji-Qing
• Journal of publication: CrystEngComm
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 3
• Pages of publication: 430
• a: 13.2295 ± 0.0008 Å
• b: 24.9102 ± 0.0017 Å
• c: 27.2377 ± 0.0019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8976.2 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 72
• Hermann-Mauguin space group symbol: I b a m
• Hall space group symbol: -I 2 2c
• Residual factor for all reflections: 0.0844
• Residual factor for significantly intense reflections: 0.0602
• Weighted residual factors for significantly intense reflections: 0.1708
• Weighted residual factors for all reflections included in the refinement: 0.1923
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No