Information card for entry 7216754

Structure parameters

• Formula: C27 H34 Cl2 N Pd Sb
• Calculated formula: C27 H34 Cl2 N Pd Sb
• SMILES: c12c(cccc1)C[N](C)(C)[Pd](Cl)(Cl)[Sb]2(c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C
• Title of publication: Palladium(ii) complexes with chiral organoantimony(iii) ligands. Solution behaviour and solid state structures
• Authors of publication: Copolovici, Dana; Isaia, Francesco; Breunig, Hans J.; Raţ, Ciprian I.; Silvestru, Cristian
• Journal of publication: RSC Advances
• Year of publication: 2014
• Journal volume: 4
• Journal issue: 51
• Pages of publication: 26569
• a: 9.3725 ± 0.0007 Å
• b: 23.1231 ± 0.0018 Å
• c: 12.9278 ± 0.001 Å
• α: 90°
• β: 107.679 ± 0.001°
• γ: 90°
• Cell volume: 2669.4 ± 0.4 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0433
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.0818
• Weighted residual factors for all reflections included in the refinement: 0.0838
• Goodness-of-fit parameter for all reflections included in the refinement: 1.137
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No