Information card for entry 7217196

Structure parameters

• Formula: C49 H61 Ge N3 O5 Ru2 Si2 Sn
• Calculated formula: C49 H61 Ge N3 O5 Ru2 Si2 Sn
• Title of publication: Steric effects in the reactions of amidinate germylenes with ruthenium carbonyl: isolation of a coordinatively unsaturated diruthenium(0) derivative
• Authors of publication: Cabeza, Javier A.; Fernández-Colinas, José M.; García-Álvarez, Pablo; Polo, Diego
• Journal of publication: RSC Advances
• Year of publication: 2014
• Journal volume: 4
• Journal issue: 59
• Pages of publication: 31503
• a: 13.0728 ± 0.0005 Å
• b: 13.3171 ± 0.0004 Å
• c: 17.1692 ± 0.0005 Å
• α: 73.514 ± 0.003°
• β: 72.315 ± 0.003°
• γ: 72.066 ± 0.003°
• Cell volume: 2649.05 ± 0.16 ų
• Cell temperature: 154 ± 2 K
• Ambient diffraction temperature: 154 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.031
• Residual factor for significantly intense reflections: 0.0248
• Weighted residual factors for significantly intense reflections: 0.0577
• Weighted residual factors for all reflections included in the refinement: 0.0622
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No