Information card for entry 7217354

Structure parameters

• Formula: C40 H40 N4 Na4 O14 Pd2
• Calculated formula: C40 H36 N4 Na4 O14 Pd2
• Title of publication: Solid-state cis‒trans isomerism in bis(oxamato)palladate(ii) complexes: synthesis, structural studies and catalytic activity
• Authors of publication: Fortea-Pérez, Francisco R.; Marino, Nadia; Armentano, Donatella; De Munno, Giovanni; Julve, Miguel; Stiriba, Salah-Eddine
• Journal of publication: CrystEngComm
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 30
• Pages of publication: 6971
• a: 16.4083 ± 0.0006 Å
• b: 22.4457 ± 0.0012 Å
• c: 13.474 ± 0.0004 Å
• α: 90°
• β: 124.48 ± 0.001°
• γ: 90°
• Cell volume: 4090.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0294
• Residual factor for significantly intense reflections: 0.0286
• Weighted residual factors for significantly intense reflections: 0.0747
• Weighted residual factors for all reflections included in the refinement: 0.0812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7216176
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No