Information card for entry 7218355

Structure parameters

• Formula: C44 H66 Cu5 N20 O93 Si2 Sm2 W22
• Calculated formula: C44 H36 Cu5 N20 O93 Si2 Sm2 W22
• Title of publication: A series of hybrids with a framework constructed from {‒SiW11‒Ln‒SiW11‒}nchains and {Cu/bimpy} ribbons
• Authors of publication: Zhou, Wanli; Zhang, Zheyu; Peng, Jun; Wang, Xiang; Shi, Zhenyu; Li, Guangzhe
• Journal of publication: CrystEngComm
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 47
• Pages of publication: 10893
• a: 11.384 ± 0.005 Å
• b: 12.189 ± 0.005 Å
• c: 23.331 ± 0.005 Å
• α: 83.75 ± 0.005°
• β: 82.022 ± 0.005°
• γ: 70.697 ± 0.005°
• Cell volume: 3019 ± 1.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.083
• Residual factor for significantly intense reflections: 0.0584
• Weighted residual factors for significantly intense reflections: 0.1584
• Weighted residual factors for all reflections included in the refinement: 0.185
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No