Information card for entry 7218883

Structure parameters

• Formula: C32 H40 Cu2 Mo12 N8 O48 P
• Calculated formula: C32 H32 Cu2 Mo12 N8 O48 P
• Title of publication: Effect of polyoxoanions and amide group coordination modes on the assembly of polyoxometalate-based metal‒organic complexes constructed from a semi-rigid bis-pyridyl-bis-amide ligand
• Authors of publication: Wang, Xiuli; Chang, Zhihan; Lin, Hongyan; Tian, Aixiang; Liu, Guocheng; Zhang, Juwen; Liu, Danna
• Journal of publication: CrystEngComm
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 4
• Pages of publication: 895
• a: 11.51 ± 0.009 Å
• b: 12.16 ± 0.01 Å
• c: 13.074 ± 0.01 Å
• α: 109.155 ± 0.013°
• β: 111.714 ± 0.012°
• γ: 96.969 ± 0.014°
• Cell volume: 1543 ± 2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.125
• Residual factor for significantly intense reflections: 0.066
• Weighted residual factors for significantly intense reflections: 0.157
• Weighted residual factors for all reflections included in the refinement: 0.1943
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No