Information card for entry 7219337

Structure parameters

• Formula: C32 H20 Cl3 F2 O6 P W
• Calculated formula: C32 H20 Cl3 F2 O6 P W
• Title of publication: Surprising behaviour of M‒CO(lone pair)⋯π(arene) interactions in the solid state of fluorinated oxaphosphirane complexes
• Authors of publication: Murcia-García, Cristina; Bauzá, Antonio; Schnakenburg, Gregor; Frontera, Antonio; Streubel, Rainer
• Journal of publication: CrystEngComm
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 8
• Pages of publication: 1769
• a: 9.9709 ± 0.0008 Å
• b: 10.8286 ± 0.0007 Å
• c: 16.093 ± 0.0015 Å
• α: 99.983 ± 0.003°
• β: 98.899 ± 0.003°
• γ: 109.619 ± 0.002°
• Cell volume: 1568.9 ± 0.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0354
• Residual factor for significantly intense reflections: 0.026
• Weighted residual factors for significantly intense reflections: 0.0524
• Weighted residual factors for all reflections included in the refinement: 0.0563
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No