Synthesis and structural characterization of six Cu(ii)-based coordination polymers using the thermally tunable 1,2,3,4-cyclobutanetetracarboxylic acid
Authors of publication
Díaz-Gallifa, P.; Fabelo, O.; Pasán, J.; Cañadillas-Delgado, L.; Ramírez, M. A.; Gallardo, A. G.; Ruiz-Pérez, C.
Journal of publication
CrystEngComm
Year of publication
2015
Journal volume
17
Journal issue
27
Pages of publication
5081
a
6.234 ± 0.0012 Å
b
11.118 ± 0.002 Å
c
11.948 ± 0.002 Å
α
86.78 ± 0.03°
β
79.95 ± 0.03°
γ
83.01 ± 0.03°
Cell volume
808.8 ± 0.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0719
Residual factor for significantly intense reflections
0.0615
Weighted residual factors for significantly intense reflections
0.1767
Weighted residual factors for all reflections included in the refinement
0.1912
Goodness-of-fit parameter for all reflections included in the refinement
