Information card for entry 7220798

Structure parameters

• Formula: Fe4 H92 Lu2 O112 Sb2 W18
• Calculated formula: Fe4 Lu2 O112 Sb2 W18
• Title of publication: The first purely inorganic polyoxotungstates constructed from dimeric tungstoantimonate-based iron‒rare-earth heterometallic fragments
• Authors of publication: Chen, Lijuan; Cao, Jing; Li, Xinghua; Ma, Xing; Luo, Jie; Zhao, Junwei
• Journal of publication: CrystEngComm
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 27
• Pages of publication: 5002
• a: 12.7131 ± 0.0016 Å
• b: 12.9743 ± 0.0017 Å
• c: 15.96 ± 0.002 Å
• α: 75.09 ± 0.002°
• β: 74.312 ± 0.002°
• γ: 75.818 ± 0.002°
• Cell volume: 2405.2 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0522
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.1106
• Weighted residual factors for all reflections included in the refinement: 0.1157
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No