Cobalt(ii/iii), nickel(ii) and copper(ii) coordination clusters employing a monoanionic Schiff base ligand: synthetic, topological and computational mechanistic aspects
Authors of publication
Loukopoulos, Edward; Berkoff, Benjamin; Griffiths, Kieran; Keeble, Victoria; Dokorou, Vassiliki N.; Tsipis, Athanassios C.; Escuer, Albert; Kostakis, George E.
Journal of publication
CrystEngComm
Year of publication
2015
Journal volume
17
Journal issue
35
Pages of publication
6753
a
12.6956 ± 0.0004 Å
b
14.4449 ± 0.0004 Å
c
22.4981 ± 0.0007 Å
α
77.797 ± 0.002°
β
79.842 ± 0.002°
γ
72.698 ± 0.003°
Cell volume
3821.6 ± 0.2 Å3
Cell temperature
100 K
Ambient diffraction temperature
100 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.145
Residual factor for significantly intense reflections
0.0746
Weighted residual factors for significantly intense reflections
0.1315
Weighted residual factors for all reflections included in the refinement
0.1562
Goodness-of-fit parameter for all reflections included in the refinement
