Synthesis, characterization and theoretical calculations of model compounds of silanols catalyzed by TEMPO to elucidate the presence of Si-O-Si and Si-O-N bonds.
Authors of publication
Percino, M. Judith; Pacheco, José Alberto; Soriano, Guillermo; Ceron, Margarita; Castro, María Eugenia; Chapela, Víctor M.; bonilla-cruz, jose; Lara, Tania; Flores, Mildred; Saldivar, Enrique
Journal of publication
RSC Adv.
Year of publication
2015
a
8.5829 ± 0.0004 Å
b
9.4856 ± 0.0004 Å
c
10.9694 ± 0.0005 Å
α
95.951 ± 0.004°
β
111.779 ± 0.004°
γ
113.352 ± 0.004°
Cell volume
727.71 ± 0.07 Å3
Cell temperature
110 ± 2 K
Ambient diffraction temperature
110 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0328
Residual factor for significantly intense reflections
0.0318
Weighted residual factors for significantly intense reflections
0.0821
Weighted residual factors for all reflections included in the refinement
0.0828
Goodness-of-fit parameter for all reflections included in the refinement
