Information card for entry 7223021

Structure parameters

• Common name: COPPERR-LEAD THIOLATE
• Formula: C102 H86 Cu2 P4 Pb S5
• Calculated formula: C15.6923 H13.2308 Cu0.307692 P0.615385 Pb0.153846 S0.769231
• Title of publication: Rich Synthetic and Structural Chemistry of Polynuclear Pb(II)-Cu(I)/Ag(I) Heterobimetallic Thiolate Clusters, their Decomposition and Generation of a Cu(II) Hydrosulfide Variant.
• Authors of publication: Gupta, Geetika; Bhattacharya, Subrato
• Journal of publication: RSC Adv.
• Year of publication: 2015
• a: 12.8133 ± 0.0007 Å
• b: 13.2814 ± 0.0007 Å
• c: 30.5065 ± 0.0015 Å
• α: 100.487 ± 0.004°
• β: 90.174 ± 0.004°
• γ: 118.261 ± 0.005°
• Cell volume: 4472.4 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1155
• Residual factor for significantly intense reflections: 0.0642
• Weighted residual factors for significantly intense reflections: 0.1098
• Weighted residual factors for all reflections included in the refinement: 0.1371
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No