Synthesis and structure of new polyhedral Ni, Na- and Cu, Na-metallasiloxanes with tolyl substituent at the silicon atom
Authors of publication
Anisimov, Anton A.; Kononevich, Yuriy N.; Zhemchugov, Pavel V.; Milenin, Sergey A.; Korlyukov, Alexander A.; Tsareva, Ul'yana S.; Peregudov, Alexander S.; Dorovatovskii, Pavel V.; Molodtsova, Yuliya A.; Takazova, Rina U.; Shchegolikhina, Olga I.; Muzafarov, Aziz M.
Journal of publication
RSC Adv.
Year of publication
2016
Journal volume
6
Journal issue
26
Pages of publication
22052
a
12.919 ± 0.0006 Å
b
13.675 ± 0.0006 Å
c
23.8149 ± 0.0011 Å
α
76.271 ± 0.0011°
β
77.6651 ± 0.0011°
γ
74.0613 ± 0.001°
Cell volume
3880 ± 0.3 Å3
Cell temperature
120 K
Ambient diffraction temperature
120 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1656
Residual factor for significantly intense reflections
0.0771
Weighted residual factors for significantly intense reflections
0.146
Weighted residual factors for all reflections included in the refinement
0.1851
Goodness-of-fit parameter for all reflections included in the refinement
