Information card for entry 7224696

Structure parameters

• Formula: C24 H89 N16 Ni4 O50 P V18
• Calculated formula: C24 H74 N16 Ni4 O50 P V18
• Title of publication: Supermolecular assembly of polyoxoanion and metal-organic cationic units towards model of core‒shell nanostructure
• Authors of publication: zhou, Yang-Yang; Kong, Ya-jie; Jia, Qianqian; Yao, shuang; Yan, Jinghui
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 11.7978 ± 0.0009 Å
• b: 26.8599 ± 0.0019 Å
• c: 23.7929 ± 0.0017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7539.7 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.1076
• Residual factor for significantly intense reflections: 0.0729
• Weighted residual factors for significantly intense reflections: 0.1484
• Weighted residual factors for all reflections included in the refinement: 0.1666
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No