Information card for entry 7225404

Structure parameters

• Formula: C30 H64 N10 Ni O17 S2
• Calculated formula: C28 H46 N10 Ni O10 S2
• Title of publication: Reaction of sodium 2-(2-(2,4-dioxopentan-3-ylidene)hydrazinyl) benzenesulfonate with ethylenediamine on Cu(II) and Ni(II) centres: efficient Cu(II) homogeneous catalysts for cyanosilylation of aldehydes
• Authors of publication: Mahmoud, Abdallah G.; Mahmudov, Kamran T.; Guedes da Silva, M. Fátima C.; Pombeiro, Armando J. L.
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 11.5824 ± 0.0007 Å
• b: 13.5921 ± 0.0007 Å
• c: 14.6115 ± 0.0009 Å
• α: 72.171 ± 0.003°
• β: 75.626 ± 0.004°
• γ: 85.53 ± 0.003°
• Cell volume: 2121.2 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1335
• Residual factor for significantly intense reflections: 0.0604
• Weighted residual factors for significantly intense reflections: 0.1469
• Weighted residual factors for all reflections included in the refinement: 0.1705
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No