Information card for entry 7226169

Structure parameters

• Chemical name: Tetranitratobis(2-acetylpyridylnicotinylhydrozone)dilead(II))
• Formula: C13 H12 N6 O7 Pb
• Calculated formula: C13 H12 N6 O7 Pb
• SMILES: [Pb]123(ON(=[O]1)=O)(ON(=O)=O)[O]=C(N[N]3=C(c1[n]2cccc1)C)c1cnccc1
• Title of publication: Metal‒organic and supramolecular lead(ii) networks assembled from isomeric nicotinoylhydrazone blocks: the effects of ligand geometry and counter-ion on topology and supramolecular assembly
• Authors of publication: Mahmoudi, Ghodrat; Bauzá, Antonio; Frontera, Antonio; Garczarek, Piotr; Stilinović, Vladimir; Kirillov, Alexander M.; Kennedy, Alan; Ruiz-Pérez, Catalina
• Journal of publication: CrystEngComm
• Year of publication: 2016
• Journal volume: 18
• Journal issue: 28
• Pages of publication: 5375
• a: 9.0862 ± 0.0004 Å
• b: 9.3122 ± 0.0004 Å
• c: 11.5175 ± 0.0005 Å
• α: 84.905 ± 0.001°
• β: 72.809 ± 0.001°
• γ: 62.775 ± 0.001°
• Cell volume: 826.61 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0198
• Residual factor for significantly intense reflections: 0.0192
• Weighted residual factors for significantly intense reflections: 0.0484
• Weighted residual factors for all reflections included in the refinement: 0.0487
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No