Synthesis, Crystal Structure and Hydrolysis of Novel Isomeric Cage (P–C/P–O)-Phosphoranes on the basis of 4,4,5,5-Tetramethyl-2-(2-oxo-1,2-diphenylethoxy)-1,3,2-dioxaphospholane and Hexafluoroacetone
Authors of publication
Khasiyatullina, Nadezhda; Mironov, Vladimir Fedorovich; Krivolapov, Dmitry; Mironova, Ekaterina V.; Gnezdilov, Oleg I.
Journal of publication
RSC Adv.
Year of publication
2016
a
10.788 ± 0.013 Å
b
10.889 ± 0.013 Å
c
12.329 ± 0.015 Å
α
70.63 ± 0.02°
β
71.74 ± 0.02°
γ
67.883 ± 0.019°
Cell volume
1236 ± 3 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1946
Residual factor for significantly intense reflections
0.088
Weighted residual factors for significantly intense reflections
0.2734
Weighted residual factors for all reflections included in the refinement
0.3522
Goodness-of-fit parameter for all reflections included in the refinement
