Information card for entry 7227833

Structure parameters

• Common name: (Dipp-BIANF)FeCl2
• Formula: C68 H71 Cl2 F Fe N2 O3
• Calculated formula: C68 H71 Cl2 F Fe N2 O3
• Title of publication: Ferrous complexes supported by sterically encumbered asymmetric bis(arylimino)acenaphthene (BIAN) ligands: synthesis, characterization and screening for catalytic hydrosilylation of carbonyl compounds
• Authors of publication: Yu, Xun; Zhu, Feifeng; Bu, Donglei; Lei, Hao
• Journal of publication: RSC Adv.
• Year of publication: 2017
• Journal volume: 7
• Journal issue: 25
• Pages of publication: 15321
• a: 10.383 ± 0.00014 Å
• b: 21.4869 ± 0.0004 Å
• c: 25.4145 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5669.94 ± 0.15 ų
• Cell temperature: 93 K
• Ambient diffraction temperature: 93 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0959
• Weighted residual factors for all reflections included in the refinement: 0.0972
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No