A chiral spiroborate anion from diphenyl-l-tartramide [B{l-Tar(NHPh)2}2]−applied to some challenging resolutions
Authors of publication
Wong, Lawrence W.-Y.; Tam, Gemma S.-S.; Chen, Xiaoyan; So, Frederick T.-K.; Soecipto, Aristyo; Sheong, Fu Kit; Sung, Herman H.-Y.; Lin, Zhenyang; Williams, Ian D.
Journal of publication
CrystEngComm
Year of publication
2018
Journal volume
20
Journal issue
33
Pages of publication
4831
a
30.9663 ± 0.0009 Å
b
13.3119 ± 0.0004 Å
c
7.0955 ± 0.0003 Å
α
90°
β
93.965 ± 0.003°
γ
90°
Cell volume
2917.91 ± 0.17 Å3
Cell temperature
100.01 ± 0.1 K
Ambient diffraction temperature
100.01 ± 0.1 K
Number of distinct elements
5
Space group number
5
Hermann-Mauguin space group symbol
C 1 2 1
Hall space group symbol
C 2y
Residual factor for all reflections
0.0485
Residual factor for significantly intense reflections
0.0425
Weighted residual factors for significantly intense reflections
0.1147
Weighted residual factors for all reflections included in the refinement
0.117
Goodness-of-fit parameter for all reflections included in the refinement
