Information card for entry 7232249

Structure parameters

• Formula: C6 H24 N6 Ni Se12 Sn
• Calculated formula: C6 H24 N6 Ni Se12 Sn
• Title of publication: Alcohol-solvothermal syntheses, crystal structures and photocatalytic properties of tin selenides with polyselenide ligands
• Authors of publication: Han, Jingyu; Zhang, Limei; Li, Shufen; Zheng, Wei; Jia, Dingxian; Yuan, Yaxian
• Journal of publication: CrystEngComm
• Year of publication: 2019
• Journal volume: 21
• Journal issue: 10
• Pages of publication: 1642
• a: 10.104 ± 0.002 Å
• b: 12.048 ± 0.002 Å
• c: 12.107 ± 0.002 Å
• α: 89.524 ± 0.014°
• β: 75.445 ± 0.017°
• γ: 75.777 ± 0.017°
• Cell volume: 1380.5 ± 0.5 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0628
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.0732
• Weighted residual factors for all reflections included in the refinement: 0.0929
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No