Information card for entry 7232487

Structure parameters

• Formula: C16.67 H32 N6.67 Ni5 O33.67 P0.67 W6
• Calculated formula: C16.6667 H4 N6.66667 Ni5 O33.6667 P0.666667 W6
• Title of publication: Syntheses, structures and properties of three organic‒inorganic hybrid polyoxotungstates constructed from {Ni6PW9} building blocks: from isolated clusters to 2-D layers
• Authors of publication: Zhang, Zhong; Wang, Yue-Lin; Li, Hai-Lou; Sun, Ke-Ning; Yang, Guo-Yu
• Journal of publication: CrystEngComm
• Year of publication: 2019
• Journal volume: 21
• Journal issue: 16
• Pages of publication: 2641
• a: 21.5089 ± 0.0016 Å
• b: 21.5089 ± 0.0016 Å
• c: 58.751 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 23539 ± 3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0941
• Residual factor for significantly intense reflections: 0.0712
• Weighted residual factors for significantly intense reflections: 0.2003
• Weighted residual factors for all reflections included in the refinement: 0.2162
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No