Information card for entry 7232603

Structure parameters

• Formula: Mo8 O45 Tm2
• Calculated formula: Mo8 O45 Tm2
• Title of publication: Ln(iii)-Containing polyoxomolybdates based on β-{Mo8O28}: microwave synthesis and optical and magnetic properties
• Authors of publication: Zhao, Yanxin; Chen, Shumin; Ji, Yanfang; Singh, Vikram; Ma, Pengtao; Lu, Jingkun; Niu, Jingyang; Wang, Jingping
• Journal of publication: CrystEngComm
• Year of publication: 2019
• Journal volume: 21
• Journal issue: 23
• Pages of publication: 3627
• a: 9.2867 ± 0.0007 Å
• b: 10.2931 ± 0.0008 Å
• c: 10.7281 ± 0.0008 Å
• α: 90.623 ± 0.001°
• β: 99.019 ± 0.001°
• γ: 102.689 ± 0.001°
• Cell volume: 986.98 ± 0.13 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0269
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for significantly intense reflections: 0.0669
• Weighted residual factors for all reflections included in the refinement: 0.0677
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No