Information card for entry 7232945

Structure parameters

• Formula: C24 H38 N8 Ni2 O13
• Calculated formula: C24 H38 N8 Ni2 O13
• Title of publication: Variation of nuclearity in NiII complexes of a Schiff base ligand: crystal structures and magnetic studies
• Authors of publication: Ghosh, Tanmoy Kumar; Mahapatra, Prithwish; Jana, Subrata; Ghosh, Ashutosh
• Journal of publication: CrystEngComm
• Year of publication: 2019
• Journal volume: 21
• Journal issue: 31
• Pages of publication: 4620
• a: 5.1874 ± 0.0004 Å
• b: 34.715 ± 0.003 Å
• c: 18.1886 ± 0.0015 Å
• α: 90°
• β: 90.275 ± 0.002°
• γ: 90°
• Cell volume: 3275.4 ± 0.5 ų
• Cell temperature: 292 ± 2 K
• Ambient diffraction temperature: 292 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1168
• Residual factor for significantly intense reflections: 0.0806
• Weighted residual factors for significantly intense reflections: 0.1946
• Weighted residual factors for all reflections included in the refinement: 0.211
• Goodness-of-fit parameter for all reflections included in the refinement: 1.142
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No