Information card for entry 7235791

Structure parameters

• Formula: C49.28 H42.28 Cl1.45 N2.28 O P4 Se2
• Calculated formula: C49.2684 H42.2968 Cl1.4568 N2.27 O P4 Se2
• Title of publication: Synthesis of iron selenide nanocrystals and thin films from bis(tetraisopropyldiselenoimidodiphosphinato)iron(ii) and bis(tetraphenyldiselenoimidodiphosphinato)iron(ii) complexes
• Authors of publication: Akhtar, Masood; Malik, Mohammad Azad; Raftery, James; O'Brien, Paul
• Journal of publication: J. Mater. Chem. A
• Year of publication: 2014
• Journal volume: 2
• Journal issue: 48
• Pages of publication: 20612
• a: 10.7461 ± 0.0002 Å
• b: 20.0351 ± 0.0004 Å
• c: 21.4593 ± 0.0004 Å
• α: 90°
• β: 92.389 ± 0.001°
• γ: 90°
• Cell volume: 4616.15 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0317
• Residual factor for significantly intense reflections: 0.0283
• Weighted residual factors for significantly intense reflections: 0.0737
• Weighted residual factors for all reflections included in the refinement: 0.0757
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No