Mononuclear palladium and heterodinuclear palladium–ruthenium complexes of semicarbazone ligands. Synthesis, characterization, and application in C–C cross-coupling reactions
Authors of publication
Datta, Sayanti; Kumar Seth, Dipravath; Halder, Sarmistha; Sheldrick, William S.; Mayer-Figge, Heike; Drew, Michael G. B.; Bhattacharya, Samaresh
Journal of publication
RSC Advances
Year of publication
2012
Journal volume
2
Journal issue
12
Pages of publication
5254
a
10.1264 ± 0.0009 Å
b
14.1165 ± 0.0012 Å
c
16.8322 ± 0.0012 Å
α
80.414 ± 0.007°
β
84.706 ± 0.007°
γ
78.503 ± 0.007°
Cell volume
2320.6 ± 0.3 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0923
Residual factor for significantly intense reflections
0.0436
Weighted residual factors for significantly intense reflections
0.0862
Weighted residual factors for all reflections included in the refinement
0.0976
Goodness-of-fit parameter for all reflections included in the refinement
