Information card for entry 7250424

Structure parameters

• Chemical name: 20220606L2CuI100K
• Formula: C32 H48 Cu4 I4 N4 Si4
• Calculated formula: C32 H48 Cu4 I4 N4 Si4
• Title of publication: CP/MAS NMR studies on binding environment of CH3CN in Cu(i) complexes with disilane-bridged bis(methylpyridine) ligands
• Authors of publication: Sato, Kei-ichi; Hattori, Mineyuki; Yamanoi, Yoshinori
• Journal of publication: RSC Advances
• Year of publication: 2025
• Journal volume: 15
• Journal issue: 21
• Pages of publication: 16968 - 16972
• a: 9.8145 ± 0.0005 Å
• b: 14.001 ± 0.0008 Å
• c: 16.7363 ± 0.001 Å
• α: 90°
• β: 98.366 ± 0.002°
• γ: 90°
• Cell volume: 2275.3 ± 0.2 ų
• Cell temperature: 109 K
• Ambient diffraction temperature: 109 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0184
• Residual factor for significantly intense reflections: 0.0177
• Weighted residual factors for significantly intense reflections: 0.0459
• Weighted residual factors for all reflections included in the refinement: 0.0462
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No