Information card for entry 7250678

Structure parameters

• Formula: C24 H22 N O2 P
• Calculated formula: C24 H22 N O2 P
• Title of publication: Photoinduced cobaloxime catalysis enabled dehydrogenative C2-phosphinylation of bicyclo[1.1.0]butanes to access phosphorylated cyclobutenes
• Authors of publication: Chang, Yunong; Bian, Fangyu; Guo, Jiefei; Li, Miao-Miao; Ding, Wei
• Journal of publication: RSC Advances
• Year of publication: 2025
• Journal volume: 15
• Journal issue: 29
• Pages of publication: 24053 - 24057
• a: 11.5363 ± 0.0001 Å
• b: 12.0675 ± 0.0001 Å
• c: 14.5536 ± 0.0001 Å
• α: 90°
• β: 102.115 ± 0.001°
• γ: 90°
• Cell volume: 1980.95 ± 0.03 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0351
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0857
• Weighted residual factors for all reflections included in the refinement: 0.0874
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No