Information card for entry 7251957

Structure parameters

• Formula: C30 H32 N6 O9 Pb2 S
• Calculated formula: C30 H32 N6 O9 Pb2 S
• Title of publication: Dative and Noncovalent Tetrel Bonding in Hemidirected Pb(II) Complexes with Thiosemicarbazone and Hydrazone Ligands: Significance in Crystal Packing and Computational Insights into Pb•••N/S/O Interactions
• Authors of publication: Adhikari, Suman; Nath, Sourav; Kaminsky, Werner; Krajewski, Sebastian; Shukla, Rahul; Roy, Subhadip
• Journal of publication: CrystEngComm
• Year of publication: 2026
• a: 11.4145 ± 0.0003 Å
• b: 15.5121 ± 0.0005 Å
• c: 18.7691 ± 0.0006 Å
• α: 90°
• β: 100.922 ± 0.002°
• γ: 90°
• Cell volume: 3263.11 ± 0.17 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0575
• Residual factor for significantly intense reflections: 0.0356
• Weighted residual factors for significantly intense reflections: 0.0816
• Weighted residual factors for all reflections included in the refinement: 0.0889
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No