Information card for entry 7700086

Structure parameters

• Formula: C89 H67 B Cl9 F24 O2 P4 Rh
• Calculated formula: C89 H67 B Cl9 F24 O2 P4 Rh
• Title of publication: Synthesis and characterization of rhodium-aluminum heterobimetallic complexes tethered by a 1,3-bis(diphenylphosphino)-2-propanoxy group.
• Authors of publication: Li, Zhongjing; Yokley, Timothy W.; Tran, Sheila L.; Zong, Jie; Schley, Nathan D.; Brewster, Timothy P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 24
• Pages of publication: 8782 - 8790
• a: 11.4257 ± 0.0006 Å
• b: 19.1875 ± 0.001 Å
• c: 22.2983 ± 0.001 Å
• α: 82.035 ± 0.004°
• β: 76.317 ± 0.004°
• γ: 79.953 ± 0.004°
• Cell volume: 4652.6 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1239
• Residual factor for significantly intense reflections: 0.0929
• Weighted residual factors for significantly intense reflections: 0.2224
• Weighted residual factors for all reflections included in the refinement: 0.2448
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No