Information card for entry 7700099

Structure parameters

• Formula: C6 H24 Cl Co N4 O8
• Calculated formula: C6 H24 Cl Co N4 O8
• Title of publication: The synthesis, structure and catalytic properties of the [Mo₇O₂₄(μ-Mo₈O₂₆)Mo₇O₂₄]^16- anion formed via two intermediate heptamolybdates [Co(en)₃]₂[NaMo₇O₂₄]Cl·nH₂O and (H₃O)[Co(en)₃]₂[Mo₇O₂₄]Cl·9H₂O.
• Authors of publication: Damjanović, Vladimir; Pisk, Jana; Kuzman, Dino; Agustin, Dominique; Vrdoljak, Višnja; Stilinović, Vladimir; Cindrić, Marina
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 27
• Pages of publication: 9974 - 9983
• a: 6.332 ± 0.0003 Å
• b: 11.9658 ± 0.0005 Å
• c: 20.2599 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1535.04 ± 0.13 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0435
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0655
• Weighted residual factors for all reflections included in the refinement: 0.0669
• Goodness-of-fit parameter for all reflections included in the refinement: 0.935
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No