Information card for entry 7700110

Structure parameters

• Formula: C92 H112 F48 N12 P8 Rh4
• Calculated formula: C92 H112 F48 N12 P8 Rh4
• Title of publication: Structural and chemical properties of half-sandwich rhodium complexes supported by the bis(2-pyridyl)methane ligand.
• Authors of publication: Lionetti, Davide; Day, Victor W.; Blakemore, James D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12396 - 12406
• a: 16.7908 ± 0.0007 Å
• b: 15.7747 ± 0.0006 Å
• c: 10.9869 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2910.1 ± 0.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 199.99 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0408
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for significantly intense reflections: 0.0831
• Weighted residual factors for all reflections included in the refinement: 0.0867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No