Information card for entry 7700277

Structure parameters

• Formula: C40 H82 Cl2 N2 P2 Si8
• Calculated formula: C40 H82 Cl2 N2 P2 Si8
• Title of publication: [E(μ-NBbp)]₂ (E = P, As) - group 15 biradicals synthesized from acyclic precursors.
• Authors of publication: Bresien, Jonas; Schulz, Axel; Szych, Lilian Sophie; Villinger, Alexander; Wustrack, Ronald
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 29
• Pages of publication: 11103 - 11111
• a: 13.3218 ± 0.0009 Å
• b: 15.5388 ± 0.0011 Å
• c: 14.3474 ± 0.001 Å
• α: 90°
• β: 112.395 ± 0.002°
• γ: 90°
• Cell volume: 2746 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0793
• Residual factor for significantly intense reflections: 0.0401
• Weighted residual factors for significantly intense reflections: 0.0737
• Weighted residual factors for all reflections included in the refinement: 0.0859
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No