Information card for entry 7700292

Structure parameters

• Formula: C21 H8 Cu2 Dy I2 N4 O7
• Calculated formula: C21 H8 Cu2 Dy I2 N4 O7
• Title of publication: Copper(i) iodide cluster-based lanthanide organic frameworks: synthesis and application as efficient catalysts for carboxylative cyclization of propargyl alcohols with CO₂ under mild conditions.
• Authors of publication: Wu, Zhilei; Lan, Xingwang; Zhang, Yaxin; Li, Meng; Bai, Guoyi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 29
• Pages of publication: 11063 - 11069
• a: 25.367 ± 0.0004 Å
• b: 25.367 ± 0.0004 Å
• c: 9.0667 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5834.28 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 122
• Hermann-Mauguin space group symbol: I -4 2 d
• Hall space group symbol: I -4 2bw
• Residual factor for all reflections: 0.0322
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.0635
• Weighted residual factors for all reflections included in the refinement: 0.0647
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No