Information card for entry 7700417

Structure parameters

• Formula: C34 H45 Cl2 N2 Pd2 Sb
• Calculated formula: C34 H45 Cl2 N2 Pd2 Sb
• Title of publication: Antimony(i) →Pd(ii) complexes with the (μ-Sb)Pd₂ coordination framework.
• Authors of publication: Kořenková, Monika; Hejda, Martin; Jirásko, Robert; Block, Theresa; Uhlík, Filip; Jambor, Roman; RůŽička, Aleš; Pöttgen, Rainer; Dostál, Libor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 31
• Pages of publication: 11912 - 11920
• a: 9.9651 ± 0.001 Å
• b: 22.9 ± 0.0014 Å
• c: 18.0049 ± 0.0013 Å
• α: 90°
• β: 118.278 ± 0.007°
• γ: 90°
• Cell volume: 3618.4 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0362
• Residual factor for significantly intense reflections: 0.0242
• Weighted residual factors for significantly intense reflections: 0.0514
• Weighted residual factors for all reflections included in the refinement: 0.059
• Goodness-of-fit parameter for all reflections included in the refinement: 1.212
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No