Information card for entry 7700433

Structure parameters

• Formula: Cl6 Rb3 Sc
• Calculated formula: Cl6 Rb3 Sc
• Title of publication: Two new derivatives of scandium borohydride, MSc(BH₄)₄, M = Rb, Cs, prepared via a one-pot solvent-mediated method.
• Authors of publication: Starobrat, Agnieszka; Jaroń, Tomasz; Grochala, Wojciech
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 31
• Pages of publication: 11829 - 11837
• a: 10.6873 ± 0.001 Å
• b: 10.6873 ± 0.001 Å
• c: 10.6873 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1220.7 ± 0.2 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 3
• Space group number: 225
• Hermann-Mauguin space group symbol: F m -3 m
• Hall space group symbol: -F 4 2 3
• Residual factor for all reflections: 0.0934
• Residual factor for significantly intense reflections: 0.0524
• Weighted residual factors for all reflections: 0.0632
• Weighted residual factors for significantly intense reflections: 0.0551
• Goodness-of-fit parameter for all reflections: 0.06
• Method of determination: powder diffraction
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No