Information card for entry 7700663

Structure parameters

• Formula: C34 H86 Fe Ge9 O2 Si12
• Calculated formula: C34 H86 Fe Ge9 O2 Si12
• Title of publication: The influence of the FeCp(CO)₂⁺ moiety on the dynamics of the metalloid [Ge₉(Si(SiMe₃)₃)₃]^- cluster in thf: synthesis and characterization by time-resolved absorption spectroscopy.
• Authors of publication: Michenfelder, Nadine C.; Gienger, Christian; Schnepf, Andreas; Unterreiner, Andreas-Neil
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 41
• Pages of publication: 15577 - 15582
• a: 9.5603 ± 0.0005 Å
• b: 14.6941 ± 0.0008 Å
• c: 24.4867 ± 0.0013 Å
• α: 89.905 ± 0.002°
• β: 85.864 ± 0.002°
• γ: 78.757 ± 0.002°
• Cell volume: 3364.8 ± 0.3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150.01 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0646
• Residual factor for significantly intense reflections: 0.0356
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0859
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No