Information card for entry 7700750

Structure parameters

• Common name: [GeH(N3Dmp2)]
• Formula: C51.5 H55 Ge N3
• Calculated formula: C51.5 H55 Ge N3
• Title of publication: Kinetic stabilization of low-oxidation state and terminal hydrido main group metal complexes by a sterically demanding N,N'-bis(2,6-terphenyl)triazenide.
• Authors of publication: Leverett, Anthony R.; Diachenko, Vera; Cole, Marcus L.; McKay, Alasdair I.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 35
• Pages of publication: 13197 - 13204
• a: 10.427 ± 0.0012 Å
• b: 11.3856 ± 0.0013 Å
• c: 20.013 ± 0.002 Å
• α: 104.001 ± 0.003°
• β: 93.794 ± 0.003°
• γ: 110.694 ± 0.003°
• Cell volume: 2126.3 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 149.9 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.114
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.1384
• Weighted residual factors for all reflections included in the refinement: 0.1665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No