Synthesis, structure and magnetic properties of a novel high-nuclearity oxo-carboxylate [Zn<sub>x</sub>Co<sub>13-x</sub>(μ<sub>4</sub>-O)<sub>4</sub>(O<sub>2</sub>CPh)<sub>18</sub>] cluster.
Authors of publication
Nawrocki, Jan; Prochowicz, Daniel; Justyniak, Iwona; van Leusen, Jan; Kornowicz, Arkadiusz; Kögerler, Paul; Lewiński, Janusz
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2019
Journal volume
48
Journal issue
34
Pages of publication
12828 - 12831
a
22.1339 ± 0.0005 Å
b
22.1339 ± 0.0005 Å
c
26.645 ± 0.0006 Å
α
90°
β
90°
γ
120°
Cell volume
11304.8 ± 0.4 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
5
Space group number
146
Hermann-Mauguin space group symbol
R 3 :H
Hall space group symbol
R 3
Residual factor for all reflections
0.0682
Residual factor for significantly intense reflections
0.0512
Weighted residual factors for significantly intense reflections
0.1351
Weighted residual factors for all reflections included in the refinement
0.1471
Goodness-of-fit parameter for all reflections included in the refinement
