Information card for entry 7700773

Structure parameters

• Formula: C46 H52 Cl N2 O4 P2 Re
• Calculated formula: C44 H44 Cl N2 O2 P2 Re
• Title of publication: Steric influence of salicylaldehyde-based Schiff base ligands on the formation of trans-[Re(PR₃)₂(Schiff base)]⁺ complexes.
• Authors of publication: Baumeister, Jakob E.; Mitchell, Andrew W.; Kelley, Steven P.; Barnes, Charles L.; Jurisson, Silvia S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 34
• Pages of publication: 12943 - 12955
• a: 10.5691 ± 0.0006 Å
• b: 12.4434 ± 0.0008 Å
• c: 17.0828 ± 0.001 Å
• α: 100.042 ± 0.001°
• β: 91.437 ± 0.001°
• γ: 106.144 ± 0.001°
• Cell volume: 2118.6 ± 0.2 ų
• Cell temperature: 223 K
• Ambient diffraction temperature: 223 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0503
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.0667
• Weighted residual factors for all reflections included in the refinement: 0.0722
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No