Information card for entry 7700785

Structure parameters

• Formula: C36 H16 B2 F18 N2
• Calculated formula: C36 H16 B2 F18 N2
• Title of publication: Reactions of hydrazones and hydrazides with Lewis acidic boranes.
• Authors of publication: Gazis, Theodore A.; Dasgupta, Ayan; Hill, Michael S.; Rawson, Jeremy M.; Wirth, Thomas; Melen, Rebecca L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12391 - 12395
• a: 15.7866 ± 0.0008 Å
• b: 9.641 ± 0.0004 Å
• c: 22.4406 ± 0.0011 Å
• α: 90°
• β: 108.694 ± 0.006°
• γ: 90°
• Cell volume: 3235.2 ± 0.3 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0467
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0874
• Weighted residual factors for all reflections included in the refinement: 0.0948
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No